International Journal of Scientific and Research Publications

IJSRP, Volume 4, Issue 3, March 2014 Edition [ISSN 2250-3153]

X-ray Peak Broadening Analysis of ZnO Nanoparticles Derived by Precipitation method
      Hiten Sarma, K.C. Sarma
Abstract: In the present report ZnO nanocrystals were prepared by precipitation method from Zinc Chloride and Ammonia in aqueous solutions at a pH value 8.0 .ZnO nanocrystals were then synthesized by heating the precursor in a muffle furnace at temp 350°C for 3 hours and allowed to cool to room temperature. The obtained ZnO nanoparticles have been studied using characterization techniques like X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), and Energy dispersive analysis Of X-ray (EDAX). XRD results reveal that the sample is crystalline with a hexagonal wurtzite phase. X-ray peak broadening analysis was used to evaluate the crystallite sizes and lattice strain by the Williamson-Hall (W-H) analysis. Further appropriate physical parameters such as strain, stress, and energy density values were also calculated using W-H analysis with different models, viz, uniform deformation model, uniform deformation stress model and uniform deformation energy density model. SEM and EDAX study confirms the preparation of ZnO nanoparticles.

Reference this Research Paper (copy & paste below code):

Hiten Sarma, K.C. Sarma (2018); X-ray Peak Broadening Analysis of ZnO Nanoparticles Derived by Precipitation method; Int J Sci Res Publ 4(3) (ISSN: 2250-3153). http://www.ijsrp.org/research-paper-0314.php?rp=P272451
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